Picolyl chloride → 2-({2-[2-(5-Nitrofuran-2-yl)ethenyl]-1H-imidazol-1-yl}methyl)pyridine

Participants

Role	Name	HCID	Charge
Reactant	Picolyl chloride	HCID 23393	—
Reactant	2-[2-(5-Nitro-2-furyl)vinyl]imidazole	HCID 286751	—
Product	2-({2-[2-(5-Nitrofuran-2-yl)ethenyl]-1H-imidazol-1-yl}methyl)pyridine	HCID 54275961	—

Reaction Steps

Using the same general procedure of Example 1, the captioned compound was prepared using 2-picolyl chloride and 2-[2-(5-nitro-2-furyl)vinyl]imidazole. The resulting yellow product was recrystallized from benzene-petroleum ether and melted at 141°-142°.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US03993643
Source dataset	uspto-grants-1976_11
ORD ID	ord-95bf728e56d24defb8d8211077171fc3
Source note	uspto-grants-1976_11