HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 54303272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 53940808 | HCID 53940808 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54303272 | HCID 54303272 | 57% |
Reaction Steps
The difficultly soluble isomer of [1-(2'-fluoro-4-biphenylyl)-ethylsulfinyl]-acetic acid dimethylamide was prepared analogous to Example 51 from [1-(2'-fluoro-4 -biphenylyl)-ethylthio]-acetic acid dimethylamide by oxidation with hydrogen peroxide in glacial acetic acid. Yield: 57% of theory; m.p. 131°-133° C (from toluene)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03993683 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-a517c60c66094298b34e8c16e74dad63 |
| Source note | uspto-grants-1976_11 |