Hydrogen Peroxide → HCID 54430564, compound

Participants

Reaction Steps

A suspension of 2.0 gm (6.1 millimols) of [2-(4-biphenylyl)-2-oxo-ethylthio]-acetic acid isopropylamide in 20 ml of glacial acetic acid was admixed with 1.3 ml of 30% hydrogen peroxide, and the mixture was stirred at room temperature for 2 hours. The reaction product was precipitated with water and recrystallized from ethyl acetate after drying. Yield: 71.4% of theory; m.p. 138°-1/3°C.

Provenance & Evidence