HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → 7-Chloro-5-(2-chlorophenyl)-1-methyl-[1,2,4]triazolo[4,3-A]quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | 6-Chloro-4-(2-chlorophenyl)-2-hydrazinylquinoline | HCID 21488620 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 7-Chloro-5-(2-chlorophenyl)-1-methyl-[1,2,4]triazolo[4,3-A]quinoline | HCID 21488587 | — |
Reaction Steps
In the manner given in Preparation 5, 6-chloro-2-hydrazino-4-(o-chlorophenyl)quinoline and triethyl orthoacetate in xylene were refluxed to give 7-chloro-1-methyl-5-(o-chlorophenyl)-s-triazolo[4,3-a]quinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03993660 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-a106a269e2cd413ab5b6753e51f53205 |
| Source note | uspto-grants-1976_11 |