huagongshe.com
HRID1730765

反应详情

EQUATION

反应方程式

HRID 1730765 的结构方程式

REACTANTS

反应物

2
结构：C=O
HCID712

Formaldehyde

CH2O

结构：Cc1nncn1-c1ccc(Cl)cc1C(=O)c1ccccc1Cl
HCID626552

2',5-Dichloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone

C16H11Cl2N3O

PRODUCTS

生成物

1
结构：Cc1nnc(CO)n1-c1ccc(Cl)cc1C(=O)c1ccccc1Cl
HCID6452950

2',5-Dichloro-2-(3-hydroxymethyl-5-methyl-4H-1,2,4-triazol-4-yl)benzophenone

C17H13Cl2N3O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

In the manner given in Preparation 7, 2',5-dichloro-2-(3-methyl-4H-1,2,4-triazol-4 -yl)benzophenone was treated at 125° C. in xylene with paraformaldehyde to give 2',5-dichloro-2-[3-(hydroxymethyl)-5-methyl-4H-1,2,4-triazol-4-yl] benzophenone of melting point 193.5°-195° C.