HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 21496163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 21496135 | HCID 21496135 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21496163 | HCID 21496163 | — |
Reaction Steps
In the manner given in Example 5, a solution of 5-isopropylsulfonyl-2'-fluoro-2-[3-(phthalimidomethyl)-5-propyl-4H-1,2,4-triazol-4-yl]benzophenone in methanol was heated with hydrazine hydrate to give 1-propyl-8-isopropylsulfonyl-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a][1,4]-benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03993660 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-03b8e49669934aaeb80386aa95b3046f |
| Source note | uspto-grants-1976_11 |