HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl hypochlorite → HCID 70636150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | HCID 70635455 | HCID 70635455 | — |
| Reactant | HCID 178418348 | HCID 178418348 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70636150 | HCID 70636150 | — |
Reaction Steps
In accordance with the procedures described by Example 1, benzhydryl 3-methoxymethyl-7-[2-(2-thienyl)acetamido]-3-cephem-4-carboxylate was reacted at a temperature of -80° C. with methyl lithium in the presence of methanol and t-butyl hypochlorite to provide benzhydryl 3-methoxymethyl-7-methoxy-7-[2-(2-thienyl)acetamido]-3-cephem-4-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994885 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-33ddf1ee8a5249d489b2ab2800dd2232 |
| Source note | uspto-grants-1976_11 |