Butylamine → HCID 86734218, compound

HRID 1730880Notes

Reaction equation

HRID 1730880 reaction equation
N1CCCC1.C(N)CCC.N1(C2C=CC3N(C(=O)NN=3)N=2)CCCC1.[N:26]1([C:31]2[CH:32]=[CH:33][C:34]3[N:35]([C:37](=O)[N:38]([CH2:40][CH3:41])[N:39]=3)[N:36]=2)[CH2:30][CH2:29][CH2:28][CH2:27]1>>[N:26]1([C:31]2[CH:32]=[CH:33][C:34]3[N:35]([CH2:37][N:38]([CH2:40][CH3:41])[N:39]=3)[N:36]=2)[CH2:27][CH2:28][CH2:29][CH2:30]1

Participants

5

Reactant 4

HCID 8007ButylamineHCID 31268PyrrolidineHCID 21494311HCID 21494311, compoundHCID 21494317HCID 21494317, compound

Product 1

HCID 86734218HCID 86734218, compound

Procedure

By substituting pyrrolidine for the butylamine in the procedure of Example 3 and then continuing with the procedure of Example 4, 6-pyrrolidino-1,2,4-triazolo[4,3-b]pyridazin-3(2H)-one and 6-pyrrolidino-2-ethyl-1,2,4-triazolo[4,3-b]-pyridazin-3(2H)-one, respectively, are obtained.

Workup

  1. customrespectively, are obtained

Sources & evidence

ORD record
ord-768e8812c136489cb6a3d5d8a95b1c31
Source dataset
uspto-grants-1976_11
Patent number
US03994898

Reaction notes

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