HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-3-phenyl-1H-indazole → 1-Dimethylaminoethyl-3-phenyl-5-chloroindazole hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-3-phenyl-1H-indazole | HCID 615118 | — |
| Reactant | N,N-Dimethylaminoethyl chloride hydrochloride | HCID 11636816 | — |
| Product | 1-Dimethylaminoethyl-3-phenyl-5-chloroindazole hydrochloride | HCID 68141476 | 104.2% |
Reaction Steps
By the procedure similar to that described in Example 1, 3-phenyl-5-chloroindazole (4.57 g) and dimethylaminoethyl chloride hydrochloride (4.32 g) were treated to obtain 3.5 g of 1-dimethylaminoethyl-3-phenyl-5-chloroindazole hydrochloride (m.p. 200°-201° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994890 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-e0b14f037dec4fb08b4d46ba342c6f5e |
| Source note | uspto-grants-1976_11 |