HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 68139879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 86734223 | HCID 86734223 | — |
| Product | HCID 68139879 | HCID 68139879 | 74.4% |
Reaction Steps
By the procedure similar to that described in Example 27, 1-carbamoylethyl-3-phenyl-5-chloroindazole (m.p. 156°-157° C) (5.0 g) was treated with the use of lithium aluminum hydride (1.5 g) to obtain 2.0 g of 1-aminopropyl-3-phenyl-5-chloroindazole hydrochloride having a melting point between 163°-164° C after recrystallization from ethanol-ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994890 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-ec084b82332d43f680f4b102a9557e94 |
| Source note | uspto-grants-1976_11 |