Hydrazine hydrate (1:1) → HCID 68140579, compound

HRID 1730949Notes

Reaction equation

HRID 1730949 reaction equation
C1(=O)[N:5]([CH:6]([C:9]2[CH:17]=[CH:16][CH:15]=[C:14]3[C:10]=2[C:11]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[N:12][NH:13]3)[CH2:7][CH3:8])C(=O)C2=CC=CC=C12.O.NN>>[NH2:5][CH:6]([C:9]1[CH:17]=[CH:16][CH:15]=[C:14]2[C:10]=1[C:11]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[N:12][NH:13]2)[CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 68140670HCID 68140670, compound

Product 1

HCID 68140579HCID 68140579, compoundYield 96.1%

Procedure

By the procedure similar to that described in Example 33, 1-phthalimidopropyl-3-phenylindazole (6.0 g) and hydrazine hydrate (2.0 g) were treated to obtain 3.8 g of 1-aminopropyl-3-phenylindazole as an oily product.

Workup

  1. additionwere treated

Sources & evidence

ORD record
ord-c2b420148b07489f9d6b367f87172d5a
Source dataset
uspto-grants-1976_11
Patent number
US03994890

Reaction notes

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