HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 388688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2-(4-Fluorobenzoyl)benzoic acid | HCID 82099 | — |
| Product | HCID 388688 | HCID 388688 | — |
Reaction Steps
Condense o-(p-fluorobenzoyl)benzoic acid with ethylenediamine by the procedure of Example 1 to obtain 9b-(p-fluorophenyl)-1,2,3,9b-tetrahydro-5H-imidazo[2,1-a]isoindol-5-one, reduce with lithium aluminum hydride and treat with hydrogen chloride as described in Example 1 to obtain 1-(p-fluorophenyl)-1,2,3,4,5,6-hexahydro-2,5-benzodiazocine, dihydrochloride, m.p. 303° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994920 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-13e1cc1392e743e5aedc039e5b9f42b1 |
| Source note | uspto-grants-1976_11 |