HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinemethanamine → HCID 54262084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Reactant | Methyl 2,4-bis(trifluoromethyl)benzoate | HCID 18925643 | — |
| Product | HCID 54262084 | HCID 54262084 | 64% |
Reaction Steps
5.4 g of 2,4-bis(trifluoromethyl)benzoic acid methyl ester and 2.5 g of 2-aminomethylpyridine were heated to 160°-180° C for 6 hours. After cooling, the product was recrystallized from toluene. 4.2 g (64% of theory) of N-(pyrid-2-ylmethyl)-2,4-bis(trifluoromethyl)benzoic acid amide of melting point 112°-113° C were thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03995044 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-521f76244f714722aac12e4e62bb6a2b |
| Source note | uspto-grants-1976_11 |