HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-nitrobenzoic acid → 2-Methyl-3-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-nitrobenzoic acid | HCID 16096 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2-Methyl-3-nitrobenzoyl chloride | HCID 12194872 | — |
Reaction Steps
100 g of 2-methyl-3-nitro-benzoic acid and 500 ml of thionyl chloride were refluxed for 15 hours and the mixture was then evaporated to dryness under reduced pressure to obtain 110 g of 2-methyl-3-nitro-benzoyl chloride which was used as in the synthesis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03995056 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-054a6a5718954577aa911558ed8987dc |
| Source note | uspto-grants-1976_11 |