HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzaldehyde → HCID 12801389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzaldehyde | HCID 7725 | — |
| Reactant | 1-Nitropropane | HCID 7903 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium Bisulfite | HCID 23665763 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12801389 | HCID 12801389 | — |
Reaction Steps
The procedure of Example 1 was followed for the reaction of 120 g of p-tolualdehyde and 114 g of sodium bisulfite with 178 g of 1-nitropropane and 80 g of sodium hydroxide. Water and ethanol were the solvents. The product obtained was a clear, yellow liquid weighing 100 g; ir (film) 2.8 (s), 3.4 (m), 6.5 (s), 7.3 (m), 9.7 (m), 12.2 (s) microns.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03995063 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-f0710b8b8ae84a01b59236e99ac37ff5 |
| Source note | uspto-grants-1976_11 |