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HRID1731232

反应详情

EQUATION

反应方程式

HRID 1731232 的结构方程式

REACTANTS

反应物

1
结构：COC(=O)[C@H](COC(C)(C)C)NC(=O)[C@@H](NC(=O)OCc1ccccc1)[C@@H](C)OC(C)(C)C
HCID131710554

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@H](COC(C)(C)C)NC(=O)[C@@H](N)[C@@H](C)OC(C)(C)C
HCID131710555

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

3.27 g of Z-Thr(But)-Ser(But)-OMe in 50 ml of ethyl acetate are hydrogenated in the presence of 0.5 g of palladium on charcoal (10% strength). After the absorption of hydrogen has ceased (1 hour), the catalyst is filtered off and the solution is evaporated. The product, which is obtained as an oil, is a single substance according to thin layer chromatography.

WORKUP

后处理

  1. customAfter the absorption of hydrogen
  2. custom(1 hour)
  3. filtrationthe catalyst is filtered off
  4. customthe solution is evaporated
  5. customThe product, which is obtained as an oil