HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131710559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131710561 | HCID 131710561 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131710559 | HCID 131710559 | — |
Reaction Steps
5 g of Boc-Cys(Acm)-Gly-OMe are dissolved in 20 ml of methanol and 50 ml of 4.4 N HCl in dioxane are added. After 10 minutes at 25°C, the mixture is concentrated to half its volume and 100 ml of ether are added. The mother liquor is separated from the resulting amorphous precipitate and the latter is dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994871 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-ad1ca0a550494561bd8e1207294af12b |
| Source note | uspto-grants-1976_11 |