Hydrazine → HCID 178448003, compound

Participants

Reaction Steps

A mixture of 32.6 g of p-(trans-4-(trans-4-propylcyclohexyl)-cyclohexyl)-acetophenone, 15 g of KOH, 25 ml of 85% hydrazine and 250 ml of diethylene glycol is warmed to 100° for 1 hour. The temperature is increased slowly until the hydrazone formed decomposes, and is boiled for another 4 hours, cooled and worked up in the customary manner to give trans-1-p-ethylphenyl-4-(trans-4-propylcyclohexyl)-cyclohexane.

Provenance & Evidence