HuagongsheHuagongshe Chemistry Print Report · For research reference only
Disperse Violet 1 → HCID 86741097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Disperse Violet 1 | HCID 31420 | — |
| Reactant | Cupric chloride dihydrate | HCID 61482 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86741097 | HCID 86741097 | — |
Reaction Steps
Copper (II) chloride dihydrate (0.71 g) is dissolved in dimethylformamide (30 ml) and 1,4-diamino anthraquinone (1.0 g) is added. The mixture quickly turns into a paste and is filtered and washed with methylene chloride before drying. The filtrate is then washed with water, acetone and finally methylene chloride and dried overnight in a vacuum oven. The yield is 0.86 g of a dark blue powder having a conductivity of 1.32×10-2S/cm. Analysis shows a composition of C--56.84 percent, H--3.86 percent, N--9.10 percent, Cu--5.7 percent and Cl--7.7 percent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04622169 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-4a491149d295485cba03eab6c7cf7865 |
| Source note | uspto-grants-1986_11 |