Disperse Violet 1 → HCID 86741097, compound

HRID 1731481Notes

Reaction equation

HRID 1731481 reaction equation
O.O.[Cu:3](Cl)Cl.[NH2:6][C:7]1[C:20]2[C:19](=[O:21])[C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[C:12](=[O:22])[C:11]=2[C:10]([NH2:23])=[CH:9][CH:8]=1>CN(C)C=O>[Cu+2:3].[NH2:6][C:7]1[C:20]2[C:19](=[O:21])[C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[C:12](=[O:22])[C:11]=2[C:10]([NH2:23])=[CH:9][CH:8]=1

Participants

4

Reactant 2

HCID 31420Disperse Violet 1HCID 61482Cupric chloride dihydrate

Product 1

HCID 86741097HCID 86741097, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Copper (II) chloride dihydrate (0.71 g) is dissolved in dimethylformamide (30 ml) and 1,4-diamino anthraquinone (1.0 g) is added. The mixture quickly turns into a paste and is filtered and washed with methylene chloride before drying. The filtrate is then washed with water, acetone and finally methylene chloride and dried overnight in a vacuum oven. The yield is 0.86 g of a dark blue powder having a conductivity of 1.32×10-2S/cm. Analysis shows a composition of C--56.84 percent, H--3.86 percent, N--9.10 percent, Cu--5.7 percent and Cl--7.7 percent.

Workup

  1. filtrationis filtered
  2. washwashed with methylene chloride
  3. custombefore drying
  4. washThe filtrate is then washed with water, acetone and finally methylene chloride
  5. customdried overnight in a vacuum oven

Sources & evidence

ORD record
ord-4a491149d295485cba03eab6c7cf7865
Source dataset
uspto-grants-1986_11
Patent number
US04622169

Reaction notes

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