Triethylamine → HCID 86741098, compound

Participants

Reaction Steps

Nickel (II) chloride hexahydrate (0.5 g) is dissolved in dimethylformamide (25 ml) containing 1,4-diamino anthraquinone (0.5 g) and triethylamine (0.84 g). A precipitate forms and is collected and washed repeatedly with methylene chloride until the washings are colorless. The yield is 0.66 g of a dark blue-black powder having a conductivity of 4.72×10-3S/cm. Analysis shows a composition of C--59.34 percent, H--3.76 percent, N--9.38 percent, Ni--17.2 percent and Cl--2.6 percent.

Provenance & Evidence