Triethylamine → HCID 86741099, compound

Participants

Reaction Steps

Silver (I) nitrate (0.71g) is dissolved in acetonitrile (25 ml). Triethylamine (0.3 ml) and 1,4-diamino anthraquinone (0.5 g) are added and a precipitate forms immediately. The precipitate is collected and washed with acetonitrile, dimethylformamide, acetonitrile, and finally methylene chloride before drying. The yield is 0.22 g of a dark blue-black powder having a conductivity of 7.9×10-3S/cm. Analysis shows a composition of C--38.6 percent, H--2.06 percent, N--6.12 percent and Ag--40.1 percent.

Provenance & Evidence