HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenesulfonyl chloride → HCID 70455624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 1-Pyrrolidinepropanamine | HCID 31670 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 70455624 | HCID 70455624 | — |
Reaction Steps
4-Methoxybenzenesulphonylchloride (8.26 g, 0.04 mol) was added in portions with stirring to a solution of 1-(3-aminopropyl)-pyrrolidine (5.13 g, 0.04 mol) in 10% NaOH (100 ml), and the resulting mixture was stirred at room temperature for the next 24 hours. Unreacted sulphonylchloride was filtered off, and the filtrate was adjusted to pH 9,8 with dilute HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04622331 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-871e81b013334be1b1811329c14d3dc9 |
| Source note | uspto-grants-1986_11 |