Hydrochloric Acid → HCID 131714950, compound

Participants

Reaction Conditions

Reaction Steps

To a suspension of 0.2 g of the product of Example 3 in 17 ml of water was added 0.3 g of sodium hydroxide. The blue solution was heated to 60° C. for 30 minutes. After cooling to room temperature hydrochloric acid was added until the mixture was acidic. The product was extracted into ethyl acetate then chromatographed on silica gel to give 0.05 g of 3,7-di(methysulfonamido)(10H)phenoxazine, which was identified by spectroscopic analysis.

Provenance & Evidence