Methacrylonitrile → HCID 13050978, compound

Participants

Reaction Steps

As for Example 2 a 0.32 g. amount of sodium metal is dissolved in 100 ml. of absolute ethanol, then 10.0 g. of 2-chloro-6-hydrazinopyridine is added, followed by 4.8 g. of methacrylonitrile in place of acrylonitrile. The procedure of Example 2 is followed to give 9.4 g. of crude product. The material is recrystallized from dichloromethane-hexane to give the product of the Example as pale yellow crystals, m.p. 175°-176° C.

Provenance & Evidence