HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Allylhydroxylamine → HCID 178460155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Allylhydroxylamine | HCID 420841 | — |
| Reactant | HCID 20226955 | HCID 20226955 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178460155 | HCID 178460155 | — |
Reaction Steps
10 parts by weight of 2-butyryl-5-[2-(3,5-dimethylpyrazol-1-yl)-ethyl]-cyclohexane-1,3-dione and 2.5 parts by weight of allyloxyamine in 100 parts by volume of ethanol were stirred for 12 hours at room temperature. The mixture was worked up by a method similar to that described in Example 1. 8.8 parts by weight of 2-(1-allyloxyaminobutylidene)-5-[2-(3,5-dimethylpyrazol-1-yl)-ethyl]-cyclohexane-1,3-dione of nD28 =1.5329 were obtained (Compound No. 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04623381 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-fa47602b52a544c79abfd31545ed9b25 |
| Source note | uspto-grants-1986_11 |