Ethylenediamine → HCID 10583474, compound

HRID 1731762Notes

Reaction equation

HRID 1731762 reaction equation
[CH2:1]([NH2:4])[CH2:2][NH2:3].[C:5]1([CH2:11][C:12](OCC)=[O:13])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.NCC(N)(C)C>C(OCC)(=O)C>[C:5]1([CH2:11][C:12]([NH:3][CH2:2][CH2:1][NH2:4])=[O:13])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

5

Reactant 3

HCID 3301EthylenediamineHCID 7590Ethyl phenylacetateHCID 131282-Methylpropylenediamine

Product 1

HCID 10583474HCID 10583474, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The procedure of Example IX was repeated in all essential details to produce the above compound, except that equivalent amounts of ethylenediamine and ethyl phenylacetate were substituted for 1,2-diamino-2-methylpropane and ethyl acetate, respectively. The product, which was identified by NMR and IR spectroscopy, had a melting point of 37°-38° C.

Workup

  1. customto produce the above compound

Sources & evidence

ORD record
ord-4fbd2e2afa004369b6383e3c48a8dfb6
Source dataset
uspto-grants-1986_11
Patent number
US04623652

Reaction notes

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