HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 12491965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Ethyl alpha-(phenethyl)acrylate | HCID 11117162 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12491965 | HCID 12491965 | — |
Reaction Steps
26.3 g of ethyl 2-methylene-4-phenylbutyrate (1.4) and 4 g of methylamine in 150 ml of ethanol in an autoclave were heated at 80° C. for 10 hours. After cooling down, the ethanol was removed, the residue was taken up in 1N HCl, this was extracted with ether, made alkaline with sodium carbonate and again extracted, dried and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04624962 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-841653cccc004927be79159700e4b5a3 |
| Source note | uspto-grants-1986_11 |