HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → 4-Amino-5-chloro-N-(1,2-dimethyl-4-pyrazolidinyl)-2-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | 4-Amino-5-chloro-2-methoxybenzoic acid | HCID 81626 | — |
| Reactant | HCID 20226460 | HCID 20226460 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 4-Amino-5-chloro-N-(1,2-dimethyl-4-pyrazolidinyl)-2-methoxybenzamide | HCID 13746895 | — |
Reaction Steps
The title compound was prepared as described in Example 8 of U.S. Pat. No. 4,207,327 from 4-amino-5-chloro-2-methoxybenzoic acid, triethylamine, ethylchlorocarbonate and 4-amino-1,2-dimethylpyrazolidine, m.p. 169°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04624961 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-687453c25c60477f97f710c5822f4ba6 |
| Source note | uspto-grants-1986_11 |