HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Xylene → HCID 178508879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Carbonic acid-guanidine (1:1) | HCID 286947 | — |
| Product | HCID 178508879 | HCID 178508879 | — |
Reaction Steps
A mixture of ethyl-2-cyclododecanone carboxylate (4.0 g) and guanidine carbonate (3.12 g) in xylene (50 ml) was refluxed overnight; after cooling the white solid was collected by filtration, washed with water, and recrystallized from ethanol. 2.15 g of a white powder were recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04625026 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-50ffcf5965804de9a5efd745c8a85605 |
| Source note | uspto-grants-1986_11 |