HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20226665, compound → HCID 20226652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20226665 | HCID 20226665 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20226652 | HCID 20226652 | — |
Reaction Steps
The intermediate 5,8-dihydroquinoline derivative from Example 5 is dissolved in ethanol and hydrogenated over platinum catalyst. Hydrogen uptake is monitored and the reaction stopped when exactly one equivalent of hydrogen is absorbed. The catalyst is removed by filtration and the filtrate concentrated and chromatographed to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04625034 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-9c5383498e39488ba7bc33a573e6e1b6 |
| Source note | uspto-grants-1986_11 |