HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 13723408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Bis(2-oxo-3-oxazolidinyl)phosphinic chloride | HCID 152842 | — |
| Reactant | HCID 13723399 | HCID 13723399 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13723408 | HCID 13723408 | — |
Reaction Steps
The title derivative was prepared by a procedure similar to that described in Example 8 starting with 2-[(m-nitrophenyl)amino]-4-oxo-3-furoic acid (7.4 grams, 0.028 mol), BOP-Cl (7.13 grams, 0.028 mol) and aniline (2.58 ml, 0.025 mol) dissolved in 90 ml methylene chloride. Yield: 6.71 g, mp 194°-195° C. (R2 =C6H4NO2 --m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04625040 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-d2941e58985f489c9930b25946197714 |
| Source note | uspto-grants-1986_11 |