Sodium Bicarbonate → HCID 86741130, compound

HRID 1732186Notes

Reaction equation

HRID 1732186 reaction equation
[Cl:1][C:2]1[C:12]([Cl:13])=[C:11]([C:14]2[CH2:19][CH:18]([CH3:20])[CH2:17][C:16](=[O:21])[CH:15]=2)[CH:10]=[CH:9][C:3]=1[O:4][CH2:5][C:6]([OH:8])=[O:7].C(=O)(O)[O-].[Na+:26]>O>[Cl:1][C:2]1[C:12]([Cl:13])=[C:11]([C:14]2[CH2:19][CH:18]([CH3:20])[CH2:17][C:16](=[O:21])[CH:15]=2)[CH:10]=[CH:9][C:3]=1[O:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:26]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 13749105HCID 13749105, compound

Product 1

HCID 86741130HCID 86741130, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

[2,3-Dichloro-4-(5-methyl-3-oxo-1-cyclohexen-1-yl)phenoxy]acetic acid (500 mg) is dissolved by stirring and warming with 0.25 N sodium bicarbonate solution (5.4 ml). The solution is diluted to 10 ml and sterilized by filtration. All the water that is used in the preparation is pyrogen-free. The concentration of the active agent in the final solution is 5%.

Workup

  1. additionThe solution is diluted to 10 ml and sterilized by filtration

Sources & evidence

ORD record
ord-846fa0341fcd49e88e733b30eb9277a1
Source dataset
uspto-grants-1986_11
Patent number
US04625047

Reaction notes

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