Ammonia → HCID 20305834, compound

HRID 1732227Notes

Reaction equation

HRID 1732227 reaction equation
[CH2:1]([O:3][CH2:4][CH2:5][C:6]([NH2:8])=[O:7])[CH3:2].[CH3:9][N:10]([CH3:15])[CH2:11][CH2:12][CH2:13]N.N>>[CH3:9][N:10]([CH3:15])[CH2:11][CH2:12][CH2:13][NH:8][C:6](=[O:7])[CH2:5][CH2:4][O:3][CH2:1][CH3:2]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 7993N,N-Dimethyl-1,3-propanediamineHCID 21751982HCID 21751982, compound

Product 1

HCID 20305834HCID 20305834, compound

Procedure

117.2 g of (1.0 mole) of 3-ethoxypropionamide are heated with 107.3 g (1.05 mole) of 3-dimethylaminopropylamine for 6 hours in a temperature range of 145°-170° C. until the evolution of ammonia is complete. In the subsequent distillation in a high vacuum 184 g (0.91 mole=91% of the theoretical yield) of colorless liquid are obtained having a Bp0.1 of 114°-118° C.

Workup

  1. distillationIn the subsequent distillation in a high vacuum 184 g (0.91 mole=91% of the
  2. customtheoretical yield) of colorless liquid
  3. customare obtained
  4. customa Bp0.1 of 114°-118° C.

Sources & evidence

ORD record
ord-817569078b9f448589633d03fd4cbdf9
Source dataset
uspto-grants-1980_12
Patent number
US04237067

Reaction notes

Loading…