HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20305834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | HCID 21751982 | HCID 21751982 | — |
| Product | HCID 20305834 | HCID 20305834 | — |
Reaction Steps
117.2 g of (1.0 mole) of 3-ethoxypropionamide are heated with 107.3 g (1.05 mole) of 3-dimethylaminopropylamine for 6 hours in a temperature range of 145°-170° C. until the evolution of ammonia is complete. In the subsequent distillation in a high vacuum 184 g (0.91 mole=91% of the theoretical yield) of colorless liquid are obtained having a Bp0.1 of 114°-118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237067 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-817569078b9f448589633d03fd4cbdf9 |
| Source note | uspto-grants-1980_12 |