Ammonia → HCID 20305833, compound

HRID 1732229Notes

Reaction equation

HRID 1732229 reaction equation
[CH2:1]([O:5][CH2:6][CH2:7][C:8]([NH2:10])=[O:9])[CH2:2][CH2:3][CH3:4].[CH3:11][N:12]([CH3:17])[CH2:13][CH2:14][CH2:15]N.N>>[CH3:11][N:12]([CH3:17])[CH2:13][CH2:14][CH2:15][NH:10][C:8](=[O:9])[CH2:7][CH2:6][O:5][CH2:1][CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 7993N,N-Dimethyl-1,3-propanediamineHCID 21751981HCID 21751981, compound

Product 1

HCID 20305833HCID 20305833, compound

Procedure

145.2 g (1.0 mole) of 3-n-butoxypropionamide are heated with 107.3 g (1.05 mole) of 3-dimethylaminopropylamine for 8 hours in a temperature range of 150°-170° C. until the evolution of ammonia is complete. In the subsequent distillation in a high vacuum, 204 g (0.89 mole =89% of the theoretical yield) of colorless liquid are obtained having a Bp0.1 of 122° to 124° C.

Workup

  1. distillationIn the subsequent distillation in a high vacuum, 204 g (0.89 mole =89% of the
  2. customtheoretical yield) of colorless liquid
  3. customare obtained
  4. customa Bp0.1 of 122° to 124° C.

Sources & evidence

ORD record
ord-513bd2c5e0e04b7484b3676303efa194
Source dataset
uspto-grants-1980_12
Patent number
US04237067

Reaction notes

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