HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20305833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | HCID 21751981 | HCID 21751981 | — |
| Product | HCID 20305833 | HCID 20305833 | — |
Reaction Steps
145.2 g (1.0 mole) of 3-n-butoxypropionamide are heated with 107.3 g (1.05 mole) of 3-dimethylaminopropylamine for 8 hours in a temperature range of 150°-170° C. until the evolution of ammonia is complete. In the subsequent distillation in a high vacuum, 204 g (0.89 mole =89% of the theoretical yield) of colorless liquid are obtained having a Bp0.1 of 122° to 124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237067 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-513bd2c5e0e04b7484b3676303efa194 |
| Source note | uspto-grants-1980_12 |