HCID 20305920, compound → HCID 20305914, compound

HRID 1732288Notes

Reaction equation

HRID 1732288 reaction equation
[C:1]1([CH:7]([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[O:8][C:9]([C:11]([CH3:26])([O:13][C:14]2[CH:22]=[CH:21][CH:20]=[C:16]([C:17](N)=[O:18])[C:15]=2[C:23]([NH2:25])=[O:24])[CH3:12])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>O>[C:1]1([CH:7]([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)[O:8][C:9]([C:11]([CH3:12])([O:13][C:14]2[CH:22]=[CH:21][CH:20]=[C:16]3[C:17]([NH:25][C:23](=[O:24])[C:15]=23)=[O:18])[CH3:26])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 1

HCID 20305920HCID 20305920, compound

Product 1

HCID 20305914HCID 20305914, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The reaction mixture is then poured into water slowly with stirring and a white solid forms which is filtered after 30 minutes. The precipitate is collected, dissolved in dichloromethane, washed with water, dried, filtered, and concentrated in vacuo to a small volume. The crystals that form are collected and dried over P2O5 in vacuo to yield 53.82 g. of (1-diphenylmethoxycarbonyl-1-methylethoxy)phthalamide.

Workup

  1. filtrationa white solid forms which is filtered after 30 minutes
  2. customThe precipitate is collected
  3. dissolutiondissolved in dichloromethane
  4. washwashed with water
  5. customdried
  6. filtrationfiltered
  7. concentrationconcentrated in vacuo to a small volume
  8. customThe crystals that form are collected
  9. dry with materialdried over P2O5 in vacuo
  10. customto yield 53.82 g

Sources & evidence

ORD record
ord-d7feeda1de314f92a675242cd7333f48
Source dataset
uspto-grants-1980_12
Patent number
US04237128

Reaction notes

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