HCID 20305920, compound → HCID 20305914, compound

Participants

Reaction Steps

The reaction mixture is then poured into water slowly with stirring and a white solid forms which is filtered after 30 minutes. The precipitate is collected, dissolved in dichloromethane, washed with water, dried, filtered, and concentrated in vacuo to a small volume. The crystals that form are collected and dried over P2O5 in vacuo to yield 53.82 g. of (1-diphenylmethoxycarbonyl-1-methylethoxy)phthalamide.

Provenance & Evidence