HCID 13332658, compound → 3-Hydroxymethyldibenzo[b,f]thiepin 5-oxide

HRID 1732355Notes

Reaction equation

HRID 1732355 reaction equation
[OH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][C:10]3[CH:13]=[CH:14][CH:15]=[CH:16][C:9]=3[S:8][C:7]=2[CH:17]=1.[OH:18]CC1C=CC2CCC3C=CC=CC=3SC=2C=1>>[OH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][C:10]3[CH:13]=[CH:14][CH:15]=[CH:16][C:9]=3[S:8](=[O:18])[C:7]=2[CH:17]=1

Participants

3

Reactant 2

HCID 13332658HCID 13332658, compoundHCID 202555023-Hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepin

Product 1

HCID 133326573-Hydroxymethyldibenzo[b,f]thiepin 5-oxide

Procedure

Repeat the process of Example 2, substituting an equivalent quantity of 3-hydroxymethyldibenzo[b,f]-thiepin for the 3-hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepin, to obtain the title product (m.p., 146°-148° C.).

Sources & evidence

ORD record
ord-24804b3c036f4ad9b9a72da38e557d81
Source dataset
uspto-grants-1980_12
Patent number
US04237160

Reaction notes

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