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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1732355Generated: October 31, 2026

HCID 13332658, compound → 3-Hydroxymethyldibenzo[b,f]thiepin 5-oxide

https://huagongshe.com/reaction/1732355

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 13332658HCID 13332658—
Reactant3-Hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepinHCID 20255502—
Product3-Hydroxymethyldibenzo[b,f]thiepin 5-oxideHCID 13332657—

Reaction Steps

Repeat the process of Example 2, substituting an equivalent quantity of 3-hydroxymethyldibenzo[b,f]-thiepin for the 3-hydroxymethyl-10,11-dihydrodibenzo[b,f]thiepin, to obtain the title product (m.p., 146°-148° C.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04237160
Source datasetuspto-grants-1980_12
ORD IDord-24804b3c036f4ad9b9a72da38e557d81
Source noteuspto-grants-1980_12