HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyraldehyde → HCID 70543438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Product | HCID 70543438 | HCID 70543438 | 85.5% |
Reaction Steps
The procedure is carried out as described in Example 1(a) but with the use of 216 g (2 mols) of 2-aminomethylpyridine and 144 g (2 mols) isobutyraldehyde. After a reaction time of 2 hours at 35°-40° C., subsequent distillation leaves 277 g (1.71 mols) of isobutylidene-2-aminomethylpyridine; yield 85.5% of theory; b.p. 69° C./200 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04237275 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-ff3ebe4c315242f9ad531bca9eaec962 |
| Source note | uspto-grants-1980_12 |