Resorcinol → HCID 53433129, compound

HRID 1732538Notes

Reaction equation

HRID 1732538 reaction equation
[C:1]1([CH:8]=[CH:7][CH:6]=[C:4](O)[CH:3]=1)[OH:2].[Si:9](Cl)(Cl)(Cl)[Cl:10]>>[Cl:10][Si:9].[C:1]1([OH:2])[CH:8]=[CH:7][CH:6]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 5054ResorcinolHCID 24816Silicon tetrachloride

Product 1

HCID 53433129HCID 53433129, compound

Procedure

About 0.5 mol of fine granular hydrated silica, 0.5 mol of resorcinol and 1 mol of silicon tetrachloride are slowly added while agitating and keeping the temperature below the boiling temperature of the mixture for 1 to 2 hours; the reaction is complete in 2 to 8 hours, thereby producing a phenol chlorosilicon acid resinous product. To this resinous product about 0.5 mol of phenol is added while agitating for 1 to 2 hours, thereby producing an organic silicon acid resinous product. Hydrogen chloride evolves from the mixture.

Workup

  1. customfor 1 to 2 hours

Sources & evidence

ORD record
ord-23def4a3f6284029996e4df26ed7236c
Source dataset
uspto-grants-1980_12
Patent number
US04238375

Reaction notes

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