Hydrochloric Acid → HCID 53433129, compound

HRID 1732541Notes

Reaction equation

HRID 1732541 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Si:8](Cl)(Cl)(Cl)[Cl:9].Cl>>[Cl:9][Si:8].[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 996PhenolHCID 24816Silicon tetrachloride

Product 1

HCID 53433129HCID 53433129, compound

Procedure

One mol of fine granular hydrated silica, 1 mol of phenol and 1 mol of silicon tetrachloride are slowly added simultaneously while agitating for 1 to 2 hours; hydrogen chloride is evolved and the reaction is complete in 2 to 8 hours, thereby producing a phenol chlorosilicon acid reaction product. To this resinous product, 1 mol of 2-toluenesulphonic acid is slowly added while agitating for 1 to 2 hours; the reaction is complete in 2 to 8 hours, thereby producing toluene sulphonic acid phenol silicon acid resinous product, a white granular product.

Workup

  1. waitthe reaction is complete in 2 to 8 hours

Sources & evidence

ORD record
ord-c5afd9c61d07497893238bde573aff64
Source dataset
uspto-grants-1980_12
Patent number
US04238375

Reaction notes

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