Phenol → HCID 53433129, compound

HRID 1732545Notes

Reaction equation

[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Si:8](Cl)(Cl)(Cl)[Cl:9]>>[Cl:9][Si:8].[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 2

HCID 996Phenol

HCID 24816Silicon tetrachloride

Product 1

HCID 53433129HCID 53433129, compound

Procedure

About 1 mol of hydrated silicon acid, 0.25 mol of phenol and 1 mol of silicon tetrachloride are slowly added simultaneously while agitating at ambient temperature for 1 to 2 hours; the reaction is complete in 2 to 8 hours, thereby producing a phenol chlorosilicon acid resinous product. To this resinous product, about 0.25 to 6 mols of an organic diene, isoprene, are added while agitating at a temperature between the liquid state and the boiling temperature of the diene for 1 to 2 hours; the reaction is complete in 2 to 8 hours, thereby producing a vinyl phenol silicon acid resinous product.

Workup

waitthe reaction is complete in 2 to 8 hours

Sources & evidence

ORD record: ord-0b6b3c3306464f15bd4ca0a644b7f4b3
Source dataset: uspto-grants-1980_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04238375

Reaction notes

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