O-Cresol → HCID 53433129, compound
Reaction equation
[C:1]1(C)[C:6]([OH:7])=[CH:5][CH:4]=[CH:3][CH:2]=1.[Si:9](Cl)(Cl)(Cl)[Cl:10]>>[Cl:10][Si:9].[C:6]1([OH:7])[CH:1]=[CH:2][CH:3]=[CH:4][CH:5]=1Participants
3
Procedure
About 0.5 to 1 part by weight of hydrated silica, 0.5 to 2 parts by weight of cresol and 1 part by weight of silicon tetrachloride are mixed at ambient pressure and temperature for 1 to 2 hours; the reaction is complete in 2 to 8 hours, thereby producing a phenol chlorosilicon acid resinous product. The resinous product may be washed with water and filtered to remove any hydrogen chloride.
Sources & evidence
- ORD record
- ord-5aa10f9db4e4407aaca5d8aaf52c6f8b
- Source dataset
- uspto-grants-1980_12
- Patent number
- US04238375
Reaction notes
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