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HRID1732575

反应详情

EQUATION

反应方程式

HRID 1732575 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：CCOC(=O)c1ccc2cc(CCCCBr)oc2c1
HCID20303934

未命名化合物

结构：O=C1NC(=O)c2ccccc21.[K]
HCID24194345

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1ccc2cc(CCCCN3C(=O)c4ccccc4C3=O)oc2c1
HCID20303948

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

A solution of ethyl 2-(4-bromobutyl)benzofuran-6-carboxylate (3.25 g., 0.01 mole) and potassium phthalimide (2.04 g., 0.011 mole) in dimethylformamide (25 ml.) is stirred at 25°-27° C. for 18 hours. The solution is poured into water. The precipitated ethyl 2-(4-phthalimidobutyl)benzofuran-6-carboxylate is collected by filtration.

WORKUP

后处理

  1. filtrationThe precipitated ethyl 2-(4-phthalimidobutyl)benzofuran-6-carboxylate is collected by filtration