HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cumene → HCID 86737389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cumene | HCID 7406 | — |
| Reactant | [3-(Propan-2-yl)phenyl]methanol | HCID 20301459 | — |
| Reactant | Cumen hydroperoxide | HCID 53627471 | — |
| Product | HCID 86737389 | HCID 86737389 | 90% |
Reaction Steps
To a mixture of 76 g (0.5 mole) of cumene hydroperoxide, 75 g (0.5 mole) of α,α-dimethyl-m-tolylcarbinol and 15 g of cumene was added 2 g of synthetic silica-alumina, and reaction was carried out at 60° C. for 3 hours while blowing nitrogen, to obtain cumyl-m-cymylperoxide in a yield of 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04239644 |
| Source dataset | uspto-grants-1980_12 |
| ORD ID | ord-f13d77a5f6da48f5b9d60db9c6cf7fbb |
| Source note | uspto-grants-1980_12 |