Hydrochloric Acid → HCID 12717840, compound

Participants

Reaction Steps

Five ml (0.03 mol) of a 6 N hydrochloric acid solution was pipetted into a stoppered flask containing 2.21 g (0.01 mol) of tris(dimethylaminomethyl)phosphine oxide. The mixture was shaken until the fuming and exotherming subsided, allowed to stand 30 min, and then stripped of water under vacuum, leaving 3.32 g (100% yield) of tris(dimethylaminomethyl)phosphine oxide trihydrochloride as a white, crystalline solid, m.p. 228°-229° C. dec.

Provenance & Evidence