Hydrochloric Acid → HCID 12717840, compound

HRID 1732843Notes

Reaction equation

HRID 1732843 reaction equation
[ClH:1].[CH3:2][N:3]([CH2:5][P:6](=[O:15])([CH2:11][N:12]([CH3:14])[CH3:13])[CH2:7][N:8]([CH3:10])[CH3:9])[CH3:4]>O>[ClH:1].[ClH:1].[ClH:1].[CH3:10][N:8]([CH2:7][P:6](=[O:15])([CH2:11][N:12]([CH3:14])[CH3:13])[CH2:5][N:3]([CH3:2])[CH3:4])[CH3:9]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 520039HCID 520039, compound

Product 1

HCID 12717840HCID 12717840, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Five ml (0.03 mol) of a 6 N hydrochloric acid solution was pipetted into a stoppered flask containing 2.21 g (0.01 mol) of tris(dimethylaminomethyl)phosphine oxide. The mixture was shaken until the fuming and exotherming subsided, allowed to stand 30 min, and then stripped of water under vacuum, leaving 3.32 g (100% yield) of tris(dimethylaminomethyl)phosphine oxide trihydrochloride as a white, crystalline solid, m.p. 228°-229° C. dec.

Sources & evidence

ORD record
ord-d6e5264171014faa91fbc3c87526e23d
Source dataset
uspto-grants-1980_12
Patent number
US04239701

Reaction notes

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